Thermal analyzes
Calorimetry (ITC –DSC)
Responsible : François Dole
Contact : plateforme@crpp.cnrs.fr – +33 5 56 84 30 30
One ITC systems (isothermal calorimetric titration) allowing the measurement of the heat of reaction of a solution (bio-macromolecules, molecules, NPs, etc.) according to the titrating reagent added in order to determine the concentration of a chemical species, the enthalpy (delta H), entropy (delta S) and interaction constants of the reaction: Nano ITC big volume (TA Instrument, 2009)
Two DSC (Differential Scanning Calorimetry) systems for determining phase transitions, glass transition temperature (Tg) (polymers, etc.), melting and crystallization and reaction enthalpies: DSC Q2000 (TA Instrument) and a micro DSC III (SETARAM Instrumentation) for measurements in liquids.
Thermogravimetric analyses (TGA)
Responsible : Alain Derré, F. Dole
Contact : plateforme@crpp.cnrs.fr – +33 5 56 84 30 30
Two thermogravimetric set-ups allowing the measurement of the mass variation of a sample as a function of time, for a given temperature or temperature profile and in a controlled atmosphere. TGA Q50 and TGA 5500 (TA Instrument)